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S c h e m e o f a T o F a t o m - p r o b e w i t h an e n e r g y f o c u s i n g e l e c t r o s t a t i c s e c t o r f i e l d (from r e f . 2 6 ) . 5 m . T h e a c c e p t a n c e a n g l e o r e f f e c t i v e p r o b e h o l e d i a m e t e r is d e t e r m i n e d b y an e x t e r n a l l y a d j u s t a b l e a p e r t u r e o f 2 0 o r 12 m m d i a m e t e r just in f r o n t of t h e d e f l e c t o r . The evaporation voltage w i t h i n w h i c h t h e a c t u a l e x p e r i m e n t a l t i m e f o c u s i n g is b e t t e r t h a n ±2 n a n o s e c r a n g e s t o 4% o n b o t h s i d e s o f t h e n o m i n a l V e to which the deflector voltages are set.

W . M u l l e r , Z. P h y s i k , 1 3 1 , 136 ( 1 9 5 1 ) . E . W . M u l l e r , in Advances in Electronics and Electron V o l . X I I I , 8 3 , ( 1 9 6 0 ) , L. M a r t o n , E d . , A c a d e m i c P r e s s , York. 3. E . W . M u l l e r and T. T . T s o n g , Field Ion Microscopy, Principles and Applications, Elsevier, New York (1969). E . W . M u l l e r , J. A . P a n i t z and S. B. M c L a n e , R e v . S c i . I n s t r u m . , 32, 83 ( 1 9 6 8 ) . E . W . Miiller and T. T. T s o n g , Progress in Surface Science, V o l .

These species were also "imaged" by W a u g h but are most likely afterpulse a r t i ­ facts from an e x c e s s i v e l y p u l s e d , t i m e - g a t e d s i n g l e c h a n n e l p l a t e . Atom-Probe 39 A l t h o u g h t h e d e t e r m i n a t i o n o f t h e a r e a l d i s t r i b u t i o n of ion s p e c i e s t h r o u g h t h e n a r r o w c o n f i n e s of t h e p r o b e h o l e is t e d i o u s c o m p a r e d to t h e m o r e a p p e a l i n g o n e - s h o t i m a g i n g o f a l a r g e s e c t i o n o f the c r y s t a l h e m i s p h e r e b y t h e t i m e - g a t e d field d e s o r p t i o n m i c r o s c o p e , t h e r e5 s4u l t s w i t h t h e e n e r g y f o c u s e d ToF a t o m - p r o b e a r e m o r e r e l i ­ able.

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