By Uncle Fester

This publication covers in nice aspect almost all identified equipment for making LSD. Emphasis is put on utilizing botanical resources of lysergic acid similar to ergot and morning glory seeds, yet extraction of ergotamine migraine tablets is additionally lined. each recipe is gifted besides references again to the unique works within the clinical liturature. The terminology utilized in the clinical works has been clarified and simplified, yet every one technique is right to the unique paintings. furthermore, I additionally hide the creation of the psychedelic TMA-2 from simply to be had and inexpensive calamus oil. Now that sassafras oil is hard to acquire, this topic might be of serious curiosity.

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This mixture should then be heated on a steam bath for a few hours under a nitrogen atmosphere. Next, the reaction mixture should be cooled, and sulfuric acid added to it slowly until it reaches pH 3. This results in the precipitation of crude lysergic acid having a dark color. The beaker should be allowed to sit over night in the fridge to let the crystals fully form. Then the crystals of crude D-lysergic acid should be filtered out and rinsed with a little ether. These crude crystals should be transferred to a beaker, and taken up in solution with two 200 ml portions of ethyl alcohol containing a few mls of strong ammonia.

It gives very good yields of high-quality product, if two precautions are followed. The first point on which success hinges is the requirement that a rather strict stoichiometry (stoichiometry concerns the proportions of different chemicals used in reactions) be followed in both the amount of alkali reacted with the lysergic acid to form the salt of lysergic acid, and the amount of SO 3 then added to form the mixed anhydride of lysergic acid. The other key precaution is the need to maintain strictly anhydrous conditions in both the production of the S0 3 -solvent complex, and the reaction of that complex with the lysergic acid salt to produce the mixed anhydride.

To that end, the lysergic acid crystals obtained by the methods given in Chapter 5 should be dried without heating under a vacuum for about an hour. This will remove all but the water of crystallization, which poses no problem. The scale used to portion out the ingredients for this synthesis should at least be a very sensitive triple-beamer, and its accuracy should be checked using new corrosionfree brass weight standards. Atmospheric humidity is a very real threat. NaOH, KOH, and lysergic acid will all pull water from the air.

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